Microdureza según superficie, distancia y tiempo de fotopolimerización de una resina bulk-Fill: estudio in vitro
DOI:
https://doi.org/10.15517/h2wz7d17Palabras clave:
Resinas compuestas; Luces de curación dental; Materiales dentales; Dureza; Polimerización; Factores de tiempo.Resumen
Comparar la microdureza de Vickers (VHN) según la superficie, distancia y el tiempo de fotopolimerización (FP) de Tetric® N-Ceram Bulk Fill (TNCBF). Estudio in vitro realizado en 80 muestras cilíndricas (4 mm×4 mm) distribuidas al azar en 8 grupos según distancia (0 y 3 mm) y tiempo (10, 20, 30, 40 s) de FP LED 1470 mW/cm2. La profundidad de curado fue adecuada cuando el ratio de VHN triplicadas (Kg/mm²) entre superficies inferior/superior fue>0,8. El análisis estadístico se realizó con la prueba ANOVA de tres vías con post hoc de Tukey y Tamhane (p<0,05). El efecto en la VHN fue altamente significativo al análisis individual de la superficie, tiempo y distancia de FP y por interacción tiempo × distancia de FP (p<0,001). El promedio de profundidad de curado superó el 80% de VHN independientemente de la distancia y tiempo de FP. La VHN fue mayor a una distancia de 0 mm en comparación a 3 mm con 10 y 20 s de FP independientemente de la superficie (p<0,001). La VHN fue similar en todos los tiempos con 0 mm de distancia de FP (p ≥ 0,377) y aumentó a partir de 20 s con 3 mm de distancia de FP (p≤0,001). La superficie, distancia y tiempo de FP afectaron la dureza de TNCBF lo que puede repercutir en su rendimiento clínico. La profundidad de curado mediante VHN fueron favorables con la fotopolimerización con 20 s a una distancia de 0 mm para un espesor de 4 mm de TNCBF.
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Siagian J.S., Dennis D., Ikhsan T., Abidin T. Effect of Different LED Light-curing Units on Degree of Conversion and Microhardness of Bulk-fill Composite Resin. J Contemp Dent Pract 2020; 21 (6): 615-620.
Carrillo-Marcos A., Salazar-Correa G., Castro-Ramirez L., Ladera-Castaneda M., Lopez-Gurreonero C., Cachay-Criado H., et al. The Microhardness and Surface Roughness Assessment of Bulk-Fill Resin Composites Treated with and without the Application of an Oxygen-Inhibited Layer and a Polishing System: An In Vitro Study. Polymers (Basel) 2022; 14 (15): 3053. doi: 10.3390/polym14153053
Strini B.S., Marques, Joyce Figueiredo de Lima, Pereira R., Sobral-Souza D.F., Pecorari V.G.A., Liporoni P.C.S., et al. Comparative Evaluation of Bulk-Fill Composite Resins: Knoop Microhardness, Diametral Tensile Strength and Degree of Conversion. Clin Cosmet Investig Dent 2022; 14: 225-233.
Vandewalker J.P., Casey J.A., Lincoln T.A., Vandewalle K.S. Properties of dual-cure, bulk-fill composite resin restorative materials. Gen Dent 2016; 64 (2): 68-73.
Lagocka R., Jakubowska K., Chlubek D., Buczkowska-Radlinska J. Elution study of unreacted TEGDMA from bulk-fill composite (SDR Dentsply) using HPLC. Adv Med Sci 2015; 60 (2): 191-198
Grazioli G., Cuevas-Suarez C.E., Nakanishi L., Francia A., de Moraes R.R. Physicochemical characterization of two bulk fill composites at different depths. Restor Dent Endod 2021; 46 (3): e39.
Kim R.J., Son S., Hwang J., Lee I., Seo D. Comparison of photopolymerization temperature increases in internal and external positions of composite and tooth cavities in real time: Incremental fillings of microhybrid composite vs. bulk filling of bulk fill composite. J Dent 2015; 43 (9): 1093-1098.
Leprince J.G., Palin W.M., Vanacker J., Sabbagh J., Devaux J., Leloup G. Physico-mechanical characteristics of commercially available bulk-fill composites. J Dent 2014; 42 (8): 993-1000.
Sengupta A., Naka O., Mehta S.B., Banerji S. The clinical performance of bulk-fill versus the incremental layered application of direct resin composite restorations: a systematic review. Evid Based Dent 2023; 24 (3): 143-4. Epub 2023 Jul 4
Aquino Valverde A.J., Aguilar Vargas, Gina Del Pilar, Díaz Fernández J.M., Leiva Ramírez P.A., Quintanilla Labajos D.A., Atoche Socola K.J., et al. Light-curing effectiveness using led lamps: a review. Rev Cient Odontol (Lima) 2022; 10 (3): e120.
Cidreira Boaro L.C., Pereira Lopes D., de Souza, Andreia Santos Caetano, Lie Nakano E., Ayala Perez M.D., Pfeifer C.S., et al. Clinical performance and chemical-physical properties of bulk fill composites resin -a systematic review and meta-analysis. Dent Mater 2019; 35 (10): e249-e264.
Torres C.R.G., Prado T.P., Avila, Daniele Mara da Silva, Pucci C.R., Borges A.B. Influence of Light-Curing Time and Increment Thickness on the Properties of Bulk Fill Composite Resins With Distinct Application Systems. Int J Dent 2024; 2024: 2123406.
Reis A.F., Vestphal M., Amaral R.C.d, Rodrigues J.A., Roulet J., Roscoe M.G. Efficiency of polymerization of bulk-fill composite resins: a systematic review. Braz Oral Res 2017; 31(suppl 1): e59
Rosatto C.M.P., Bicalho A.A., Veríssimo C., Bragança G.F., Rodrigues M.P., Tantbirojn D., et al. Mechanical properties, shrinkage stress, cuspal strain and fracture resistance of molars restored with bulk-fill composites and incremental filling technique. J Dent 2015; 43 (12): 1519-1528.
Aggarwal N., Jain A., Gupta H., Abrol A., Singh C., Rapgay T. The comparative evaluation of depth of cure of bulk-fill composites - An in vitro study. J Conserv Dent 2019; 22 (4): 371-375.
Aldhafyan M., Al-Odayni A., Saeed W.S., Khan R., Alrahlah A. Network integrity of bulk-fill composites: Thermal stability, post-curing hardness development and acidic softening. Dent Mater J 2025; 44 (2): 201-210
Bouschlicher M.R., Rueggeberg F.A., Wilson B.M. Correlation of bottom-to-top surface microhardness and conversion ratios for a variety of resin composite compositions. Oper Dent 2004; 29 (6): 698-704.
Farahat F., Daneshkazemi A.R., Hajiahmadi Z. The Effect of Bulk Depth and Irradiation Time on the Surface Hardness and Degree of Cure of Bulk-Fill Composites. J Dent Biomater 2016; 3 (3): 284-291.
Singha A., Dhanesha A., Nair S., Patel R., Behera S., Nanda S. Pre-heating effect on micro-hardness and depth of cure for three bulk-fill composite resins: An in vitro study. Bioinformation 2024; 20 (9): 1128-1131.
Yap A.U.J., Pandya M., Toh W.S. Depth of cure of contemporary bulk-fill resin-based composites. Dent Mater J 2016; 35 (3): 503-510.
Shimokawa C., Turbino M.L., Giannini M., Braga R.R., Price R.B. Effect of Curing Light and Exposure Time on the Polymerization of Bulk-Fill Resin-Based Composites in Molar Teeth. Oper Dent 2020; 45 (3): E141-E155.
Novin Rooz M., Yousefi Jordehi A. The Effect of Shade and Thickness on the Depth of Cure of Bulk-Fill Composites with Different Viscosities. J Dent (Shiraz) 2020; 21 (4): 322-329.
Gonder H.Y., Fidan M. Effect of different polymerization times on color change, translucency parameter, and surface hardness of bulk-fill resin composites. Niger J Clin Pract 2022; 25 (10): 1751-1757.
Besegato J.F., Jussiani E.I., Andrello A.C., Fernandes R.V., Salomao F.M., Vicentin B.L.S., et al. Effect of light-curing protocols on the mechanical behavior of bulk-fill resin composites. J Mech Behav Biomed Mater 2019; 90: 381-387.
Al Nahedh H., Al-Senan D.F., Alayad A.S. The Effect of Different Light-curing Units and Tip Distances on the Polymerization Efficiency of Bulk-fill Materials. Oper Dent 2022; 47 (4): E197-E210.
Elawsya M.E., Montaser M.A., El-Wassefy N.A., Zaghloul N.M. Depth of cure of dual- and light-cure bulk-fill resin composites. Am J Dent 2022; 35 (4): 185-190.
Saati K., Khansari S., Mahdisiar F., Valizadeh S. Evaluation of Microhardness of Two Bulk-fill Composite Resins Compared to a Conventional Composite Resin on surface and in Different Depths. J Dent (Shiraz) 2022; 23 (1): 58-64.
Doni, Santosa P., Nugraheni T. Comparison of depth of cure sonic-activated bulk-fill composite, low viscosity, and high viscosity in different thickness. J Conserv Dent 2020; 23 (6): 615-618.
Alkhudhairy F.I. The effect of curing intensity on mechanical properties of different bulk-fill composite resins. Clin Cosmet Investig Dent 2017; 9: 1-6.
Jang J., Park S., Hwang I. Polymerization shrinkage and depth of cure of bulk-fill resin composites and highly filled flowable resin. Oper Dent 2015; 40 (2): 172-180.
Maghaireh G.A., Price R.B., Abdo N., Taha N.A., Alzraikat H. Effect of Thickness on Light Transmission and Vickers Hardness of Five Bulk-fill Resin-based Composites Using Polywave and Single-peak Light-emitting Diode Curing Lights. Oper Dent 2019; 44 (1): 96-107.
Hasanain F.A., Nassar H.M., Ajaj R.A. Effect of Light Curing Distance on Microhardness Profiles of Bulk-Fill Resin Composites. Polymers (Basel) 2022; 14 (3): 528. doi: 10.3390/polym14030528
Diab R.A., Yap A.U., Gonzalez M.A.G., Yahya N.A. Impact of light-curing distance on the effectiveness of cure of bulk-fill resin-based composites. Saudi Dent J 2021; 33 (8): 1184-1189.
Hasan S.A.A., Al-Shami I.Z., Al-Hamzi M.A., Alwadai G.S., Alamoudi N.A., Alqahtani S.A., et al. Evaluation of Radiant Power of the Light Curing Units Used in Clinics at Governmental and Privates Dental Faculties. Med Devices (Auckl) 2024; 17: 301-310.
Cohen J. A power primer. Psychol Bull 1992; 112 (1): 155-159.
Price R.B.T. Light Curing in Dentistry. Dent Clin North Am 2017; 61 (4): 751-778.
Fernández Godoy E., Chaple Gil A., Caviedes Thomas R., Bersezio Miranda C., Martín Casielles J., Rodríguez Martínez G., et al. Efficiency and limitations of polywave light-curing units in restorative dentistry: a systematic review. Clin Oral Investig 2025; 29 (8): 384.
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Derechos de autor 2026 María José Loayza-Gallegos, Gino Hernan Vidalón-Romo, Julissa Amparo Dulanto-Vargas.

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